GLASS DISTILLATION ASSEMBLIES
This unit typically consists of a vessel mounted in a heating bath and is provided with a condenser for the condensation of the vapours. A receiver with drain valve can also be added for collection of the condensate. The reactor vessel can be provided in cylindrical as well as spherical shapes.
| Reactor Vessel Capacity | Condenser HTA in M2 | Batch KW | Receiver Capacity |
|---|---|---|---|
| 10 Ltr | 0.20 | 3 | 2 Ltr. |
| 20 Ltr. | 0.35 | 4.5 | 5 Ltr |
| 50 Ltr | 0.50 | 6.0 | 10 Ltr. |
| 100 Ltr | 1.50 | 9.0 | 20 Ltr |
| 200 Ltr. | 1.50 | 12.0 | 20 Ltr |
The Unit has been designed by Super to suit the customer requirement of combination of versatile reaction/distillation or combination for pilot plant work. It has flexibility to work in atmospheric pressure conditions as well as under vacuum conditions.
Typical unit has jacketed reaction vessel having facility for heating and cooling both by means of heating/cooling fluids as media. The Standard system is equipped with stirrer having mechanical seal, a packed column on the side neck of vessel, reflux divider, coil type condenser and or receiver system having a product cooler, vent, drain and vacuum valves. Options of or speed variator by mechanical variator or electronic variator can be provided.
Receiver System is equipped with product cooler, vent / vacuum valve and drain valve
The above unit is available in 10 Ltr / 20 Ltr / 50 Ltr / 100 Ltr / 200 Ltr capacities with jacketed cylindrical reactor.
| Reactor Vessel Capacity | Packed Column in mm | Condenser HTA2 in M | Product Cooler2 HTA in M | Receiver Capacity | Addition Vessel |
|---|---|---|---|---|---|
| 10 Ltr | 50 x 1000 | 0.20 | 0.10 | 2 Ltr.x 2 nos | 2 Ltr |
| 20 Ltr | 80 x 1000 | 0.35 | 0.20 | 5 Ltr.x 2 nos | 5 Ltr |
| 50 Ltr | 100 x 1000 | 0.50 | 0.20 | 10 Ltr.x 2 nos | 10 Ltr |
| 100 Ltr | 150 x 1000 | 1.50 | 0.35 | 20 Ltr.x 2 nos | 20 Ltr |
| 200 Ltr | 150 X 1000 | 1.50 | 0.35 | 20 Ltr.x 2 nos | 20 Ltr |
The Unit has been designed to suit the customers requirement of combination of versatile reaction/distillation or combination for pilot plant work.
This has a flexibility of working at atmospheric pressure as well as under vacuum.
Typical unit has a reaction vessel fitted in a Metal Heating/Cooling bath having facility for heating and cooling both by means of Heating/Cooling Fluids as a media.
The Standard system is equipped with stirrer having mechanical seal,a packed column on the side neck of the vessel, reflux divider, coil type condenser and or receiver system having a product, cooler, vent, drain and vacuum valves, Options of or speed variator by machanical variator or electronic variator can be provide. Receiver System is equipped with Product Cooler, Vent / Vacuum Valve and Drain Valve.
The above units are available in 10 Ltr./20 Ltr./50 Ltr./100 Ltr./200 Ltr.Capacity with Spherical Reactor and up to 500 Ltr. capacity with Cylindrical Reactor.
| Reactor Vessel Capacity | Packed Column in mm | Condenser HTA2 in M | Product Cooler2 HTA in M | Receiver Capacity | Addition Vessel |
|---|---|---|---|---|---|
| 10 Ltr | 50 x 1000 | 0.20 | 0.10 | 2 Ltr.x 2 nos | 2 Ltr |
| 20 Ltr | 80 x 1000 | 0.35 | 0.20 | 5 Ltr.x 2 nos | 5 Ltr |
| 50 Ltr | 100 x 1000 | 0.50 | 0.20 | 10 Ltr.x 2 nos | 10 Ltr |
| 100 Ltr | 150 x 1000 | 1.50 | 0.35 | 20 Ltr.x 2 nos | 20 Ltr |
| 200 Ltr | 150 X 1000 | 1.50 | 0.35 | 20 Ltr.x 2 nos | 20 Ltr |
- Heating mantle instead of jacketed heating / cooling bath.
- Simple Drain Valve instead of flush bottom valve.
- MS PTFE lined stirrer instead of glass stirrer.
- Variable frequency drive for variable speed.
This unit is typically used for only Distillation and Fractionation under vacuum or at atmospheric pressure. Typical unit has distillation vessel fitted in a Metal Heating / Cooling bath and with a Packed column above Reflux divider and coil condensors are fitted on the packed column. Condensed material is either taken back to the vessel or to the receiver via product cooler.
The above units are available in 10 Ltr. / 20 Ltr./50 Ltr./100 Ltr./200 Ltr. capacity Spherical Vessels and upto 500 Ltr. Capacity with Cylindrical Vessel.
| Reactor Vessel Capacity | Packed Column in mm | Condenser HTA2 in M | Product Cooler2 HTA in M | Receiver Capacity | Addition Vessel |
|---|---|---|---|---|---|
| 10 Ltr | 50 x 1000 | 0.20 | 0.10 | 2 Ltr.x 2 nos | 2 Ltr |
| 20 Ltr | 80 x 1000 | 0.35 | 0.20 | 5 Ltr.x 2 nos | 5 Ltr |
| 50 Ltr | 100 x 1000 | 0.50 | 0.20 | 10 Ltr.x 2 nos | 10 Ltr |
| 100 Ltr | 150 x 1000 | 1.50 | 0.35 | 20 Ltr.x 2 nos | 20 Ltr |
| 200 Ltr | 150 X 1000 | 1.50 | 0.35 | 20 Ltr.x 2 nos | 20 Ltr |
- Heating mantle instead of jacketed heating / cooling bath.
- Simple Drain Valve instead of flush bottom valve.
The type of Typical unit is mounted on a vapour nozzle of Glass lined Reactors.
The assembly has a Glass Packed Column to enhance Distillation. Reflux Divider and Reflux Condenser with twin receiver system is to facilitate working under vacuum or at atmospheric pressure. Receiver System is equipped with Product Cooler.Vent/Vacuum Valve and Drain Valve.
